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| DC Field | Value | Language |
|---|---|---|
| dc.contributor.author | Jain, Rajeev | - |
| dc.contributor.author | Karaiya, Shrinarayan | - |
| dc.contributor.author | Yadav, Ramji Lal | - |
| dc.contributor.author | Arya, Virendra K | - |
| dc.date.accessioned | 2012-08-31T09:33:07Z | - |
| dc.date.available | 2012-08-31T09:33:07Z | - |
| dc.date.issued | 2012-09 | - |
| dc.identifier.issn | 0975-1084 (Online); 0022-4456 (Print) | - |
| dc.identifier.uri | http://hdl.handle.net/123456789/14630 | - |
| dc.description | 606-611 | en_US |
| dc.description.abstract | This study presents synthesis of 3-[4'-(substituted) sulphonamoylphenyl] azomethine indoles (SPAI) by refluxing indole-3-carboxaldehyde with sulfonamide derivatives. Electrochemical behaviour of SPAI was studied in Britton-Robinson (BR) buffer solution (pH 2.5-12.0) at dropping mercury electrode (DME) and glassy carbon electrode (GCE). Cathodic differential pulse polarographic peak was obtained at DME in pH range 2.5-6.5. Cyclic voltammogram exhibited a well defined, irreversible cathodic and anodic peak at GCE. At pH 6.5 and above, reduction peak exhibited a tendency to split into two peaks, indicating that 1H+/2e- reduction of 2-[4’-sulphonamoylphenyl]hydrazono-1,3-indanediones occurs in one 1H+ and one 2e- steps. A product of CPE was characterized by elemental and spectral analyses. | en_US |
| dc.language.iso | en_US | en_US |
| dc.publisher | NISCAIR-CSIR, India | en_US |
| dc.rights |  CC Attribution-Noncommercial-No Derivative Works 2.5 India | en_US |
| dc.source | JSIR Vol.71(09) [September 2012] | en_US |
| dc.subject | Controlled potential electrolysis (CPE) | en_US |
| dc.subject | Cyclic voltammetry | en_US |
| dc.subject | Differential pulse polarography | en_US |
| dc.subject | 3-[4'-(substituted) Sulphonamoylphenyl] azomethine indoles (SPAI) | en_US |
| dc.title | Synthesis and electrochemical behaviour of 3-[4'-(substituted) sulphonamoylphenyl] azomethine indoles | en_US |
| dc.type | Article | en_US |
| Appears in Collections: | JSIR Vol.71(09) [September 2012] | |
Files in This Item:
| File | Description | Size | Format | |
|---|---|---|---|---|
| JSIR 71(9) 606-611.pdf | 121.1 kB | Adobe PDF | View/Open |
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