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http://nopr.niscpr.res.in/handle/123456789/15708| Title: | Template synthesis and spectral speciation of nickel(II)macrocyclic complexes derived from 4-methyl-2,6-di(formyl/benzoyl) phenol and diamines |
| Authors: | Gupta, Sushil K Jain, Kalpana Kushwah, Yogendra S |
| Issue Date: | May-1999 |
| Publisher: | NISCAIR-CSIR, India |
| Abstract: | Nickel(II )macrocyclic complexes [Ni(L)Cl2].2H2O (1,2) have been synthesized from the nickel(II )-directed condensation of 4-methyl- 2,6-diformylphenol (1) or 4-methyl-2,6-dibenzoylphenol (2) with diamines [ethylenediamine(a), 1,3-diaminopropane (b) and o-phenylenediamine (c)] in ethanol in high yields. These complexes are monomeric, non-electrolytes and paramagnetic indicating a distorted octahedral geometry around nickel, which is supported by IR , electronic, ESR and magnetic susceptibility measurements. |
| Page(s): | 506-508 |
| Appears in Collections: | IJC-A Vol.38A(05) [May 1999] |
Files in This Item:
| File | Description | Size | Format | |
|---|---|---|---|---|
| IJCA 38A(5) 506-508.pdf | 569.61 kB | Adobe PDF | View/Open |
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