Please use this identifier to cite or link to this item: http://nopr.niscpr.res.in/handle/123456789/16315
Title: Phosphorus heterocycles: Part 3 - Synthesis of Δ5-1,2,3-diazaphospholins and Δ5- 1,2,3- azaoxyphospholins from hydrazones and oximes using phase transfer catalysts †
Authors: Sarma, C S
Kataky, J C S
Issue Date: Mar-1999
Publisher: NISCAIR-CSIR, India
Abstract: The phenylhydrazones 2-4 and oximes 8 of acetophenone and substituted acetophenones react with 2,4-bis( 4-methoxyphenyl)- 1,3,2,4-dithiadiphosphetane-2,4-disulphide 1 to give Δ5-1,2,3- diazaphospholins 5-7 and Δ5-1,2,3-azaoxaphospholins 9. The reaction has been attempted using a phase transfer catalyst (PTC) hexadecyl(tributyl)phosphonium bromide. The structures of the compounds are confirmed by physical and spectral data.
Page(s): 364-366
Appears in Collections:IJC-B Vol.38B(03) [March 1999]

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