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http://nopr.niscpr.res.in/handle/123456789/21194| Title: | Synthesis and characterization of highly conjugated 22-membered octaazamacrocycles and their manganese(II), copper(II), cobalt(II) and zinc(II) complexes |
| Authors: | Khan, Tahir Ali Hasan, Syed Sirajul Jahan, Nafees Mohamed, Ajax K Islam, Khan Shoukat |
| Issue Date: | Oct-2000 |
| Publisher: | NISCAIR-CSIR, India |
| Abstract: | A new series of 21-membered macrocyclic complexes [MLX2] [M=Mn(II), Co(II), Ni(II), Cu(II) and Zn(II); X=Cl or NO3] has been synthesized by template reaction of phthalaldehyde with hydrazine hydrate and 2,4-pentanedione in methanol. The over-all Geometry and stereochemistry of these complexes have been elucidated by IR, 1H NMR, EPR, UV-vis, magnetic susceptibility and conductance values. An octahedral geometry around the metal ion is suggested for all the complexes. |
| Page(s): | 1090-1092 |
| ISSN: | 0975-0975(Online); 0376-4710(Print) |
| Appears in Collections: | IJC-A Vol.39A(10) [October 2000] |
Files in This Item:
| File | Description | Size | Format | |
|---|---|---|---|---|
| IJCA 39A(10) 1090-1092.pdf | 645.95 kB | Adobe PDF | View/Open |
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