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http://nopr.niscpr.res.in/handle/123456789/21720| Title: | Electrophilic substitution of indoles : Part XXI - Further investigation on the formation of the benzazepinone skeleton |
| Authors: | Banerji, J Chatterjee, A Saha, M Mukherjee, P Kanrar, S |
| Issue Date: | Oct-2003 |
| Publisher: | NISCAIR-CSIR, India |
| Abstract: | An interesting observation was made during the electrophilic substitution of indole with 5,5-dimethyl cyclohexane 1,3-dione resulting in the synthesis of 2,3,4,5, 10,11- hexahydro-3,3-dimelhyl-11- (indo-3-yl)-dibenz-[b,f]azepine-1-one system. The reactions with 2-methyl- and 3-methyl indoles resulted in the formation of only the 1:1 product. The structures of the products have been settled on the basis of their UV, IR.1H and 13C NMR spectral studies and MS analysis. |
| Page(s): | 2573-2576 |
| ISSN: | 0975-0983(Online); 0376-4699(Print) |
| Appears in Collections: | IJC-B Vol.42B(10) [October 2003] |
Files in This Item:
| File | Description | Size | Format | |
|---|---|---|---|---|
| IJCB 42B(10) 2573-2576.pdf | 568.17 kB | Adobe PDF | View/Open |
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