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http://nopr.niscpr.res.in/handle/123456789/466| Title: | Synthesis of N-(3′,5′-dimethyl- 4′-hydroxybenzyl)- N-tosyl-3,4-dimethoxybenzyl amine |
| Authors: | Raju, B China Neelakantan, Parvathi Bhalerao, U T |
| Keywords: | N-(3′,5′-dimethyl-4′-hydroxybenzyl)-N-tosyl-3,4-di¬¬¬me¬thoxybenzyl amine;Isoindolines |
| Issue Date: | Jan-2007 |
| Publisher: | CSIR |
| IPC Code: | Int. Cl.⁸ C07C |
| Abstract: | Reaction of 4-benzyloxy-3,5-dimethyl benzyl bromide 4 and N-tosyl-3,4-dimethoxy benzyl amine 5 gives the N-(4′-benzyloxy-3′,5′-dimethylbenzyl)-N-tosyl-3,4-dimethoxybenzyl amine 6. The obtained product on debenzylation affords N-(3′,5′-dimethyl-4′-hydroxybenzyl)-N-tosyl-3,4-dimethoxybenzyl amine 7 in 94% yield, which is key intermediate in the synthesis of isoindolines. |
| Page(s): | 201-203 |
| ISSN: | 0376-4699 |
| Appears in Collections: | IJC-B Vol.46B(01) [January 2007] |
Files in This Item:
| File | Description | Size | Format | |
|---|---|---|---|---|
| IJCB 46B(1) (2007) 201-203.pdf | 131.4 kB | Adobe PDF | View/Open |
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