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http://nopr.niscpr.res.in/handle/123456789/46806| Title: | Synthesis & characterization of diorgano(chloro)tin(IV) 2-pyridylalkoxides |
| Authors: | Visalakshi, R Jain, V K Kulshreshtha, S K Rao, G S |
| Issue Date: | Sep-1989 |
| Publisher: | NISCAIR-CSIR, India |
| Abstract: | Treatment of [R2Sn(Cl)(OPri)] with 2-pyridyl alcohols in refluxing benzene affords white crystalline solids of the type [R2Sn(Cl){O(CH2)nC5H4N}] (R = Me, Et, Pn, Bun, or Ph; n = 1 or 2). These complexes have been characterized by elemental analyses and IR, 119Sn Mossbauer and NMR (1H, 13C and 119Sn) data. In chloroform solution these complexes adopt a five-coordinate geometry as revealed by NMR data, but in solid state they appear to have some degree of molecular association. |
| Page(s): | 767-770 |
| ISSN: | 0975-0975(Online); 0376-4710(Print) |
| Appears in Collections: | IJC-A Vol.28A(09) [September 1989] |
Files in This Item:
| File | Description | Size | Format | |
|---|---|---|---|---|
| IJCA 28A(9) 767-770.pdf | 2.69 MB | Adobe PDF | View/Open |
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