Synthesis, crystal structure and thermolysis kinetics of [Co(H2O)6](ClO4)2.(HMTA)2.2H2O (HMTA = hexamethylenetetramine)

Singh, Chandra Prakash; Singh, Abhishek; Nibha; Daniliuc, Constantin G; Kumar, Bharat; Singh, Gurdip; Rao, D P

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Please use this identifier to cite or link to this item: http://nopr.niscpr.res.in/handle/123456789/57487

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DC Field	Value	Language
dc.contributor.author	Singh, Chandra Prakash	-
dc.contributor.author	Singh, Abhishek	-
dc.contributor.author	Nibha	-
dc.contributor.author	Daniliuc, Constantin G	-
dc.contributor.author	Kumar, Bharat	-
dc.contributor.author	Singh, Gurdip	-
dc.contributor.author	Rao, D P	-
dc.date.accessioned	2021-06-15T07:53:47Z	-
dc.date.available	2021-06-15T07:53:47Z	-
dc.date.issued	2021-05	-
dc.identifier.issn	0975-0975(Online); 0376-4710(Print)	-
dc.identifier.uri	http://nopr.niscair.res.in/handle/123456789/57487	-
dc.description	676-681	en_US
dc.description.abstract	A new compound, [Co(H₂O)₆](ClO₄)₂.(HMTA)₂.2H₂O; HMTA = hexamethylenetetramine) has been synthesized and characterized with the assistance of X-ray crystallography, elemental analysis, FT-IR spectroscopy, TG-DTA and DSC (N₂atmosphere). Both TG data model-fitting method as well as method of model free isoconversional have been employed to observe the kinetics of thermolysis of the compound. In order to understand the effect of sudden high heat, measurements of explosion delay are undertaken at regular five unique temperatures and the kinetics of explosion has also been explored using Arrhenius equation.	en_US
dc.language.iso	en_US	en_US
dc.publisher	NISCAIR-CSIR, India	en_US
dc.rights	CC Attribution-Noncommercial-No Derivative Works 2.5 India	en_US
dc.source	IJC-A Vol.60A(05) [May 2021]	en_US
dc.subject	Cobalt compound	en_US
dc.subject	Crystal structure	en_US
dc.subject	Thermolysis	en_US
dc.subject	Kinetics of explosion	en_US
dc.title	Synthesis, crystal structure and thermolysis kinetics of [Co(H2O)6](ClO4)2.(HMTA)2.2H2O (HMTA = hexamethylenetetramine)	en_US
dc.type	Article	en_US
Appears in Collections:	IJC-A Vol.60A(05) [May 2021]

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