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http://nopr.niscpr.res.in/handle/123456789/59033| Title: | Synthesis of monodispersed palladium nanoparticle at room temperature and its catalytic activity for Suzuki-Miyaura cross-coupling reaction |
| Authors: | Roy, Subhasish Senapati, Kula Kamal Phukan, Prodeep |
| Keywords: | Pd-Nanoparticle;nano-catalyst;2-(trimethyl silyl)-ethanol;Suzuki-Miyaura;biphenyl |
| Issue Date: | Jan-2022 |
| Publisher: | NIScPR-CSIR, India |
| Abstract: | A new method has been developed for the synthesis of spherical palladium nanoparticles with narrow size distribution. Pd nanoparticles of average particle size of around 7 nm have been prepared from Pd(OAc)2 at room temperature in THF using 2-(trimethyl silyl)-ethanol (TMSE) as a reducing as well as capping agent. The catalytic activity of the Pdnanoparticles has been examined for ligand free Suzuki-Miyaura cross-coupling reaction. |
| Page(s): | 99-105 |
| ISSN: | 2583-1321 (Online); 0019-5103 (Print) |
| Appears in Collections: | IJC Vol.61(01) [January 2022] |
Files in This Item:
| File | Description | Size | Format | |
|---|---|---|---|---|
| Indian J Chem, 61, 99-105 (Jan,2022).pdf | Main Article | 1.78 MB | Adobe PDF | View/Open |
| Indian J Chem, 61, 99-105 (Jan,2022) Suppl. Data.pdf | Supplementary Data | 134.56 kB | Adobe PDF | View/Open |
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