Please use this identifier to cite or link to this item:
http://nopr.niscpr.res.in/handle/123456789/60824| metadata.dc.identifier.doi: | https://doi.org/10.56042/ijc.v61i11.68267 |
| Title: | Solvent and catalyst free efficient chemoselective synthesis of 1,1-diacetate under visible light irradiation |
| Authors: | Hote, Baliram S Siddiqui, Tabassum A J Pisal, Parshuram M |
| Keywords: | 1,1-Diacetate;Visible light;Solvent- and catalyst free |
| Issue Date: | Nov-2022 |
| Publisher: | NIScPR-CSIR, India |
| Abstract: | One of the synthetic intermediates is used in many organic transformations. A method for highly efficient synthesis of 1,1-diacetate (3a-j) from mixture of various substituted benzaldehydes and acetic anhydride under solvent- and catalyst free using visible light irradiation (150 W tungsten lamp) has been developed. The main advantages of this protocol includes shorter reaction time, eco-friendly, mild reaction condition, easy work-up procedures, high yields of products, are the attractive features of the present methodology. All synthesized 3a-j compounds were characterized by IR, 1H NMR and mass spectral analysis. |
| Page(s): | 1184-1187 |
| ISSN: | 2583-1321 (Online); 0019-5103 (Print) |
| Appears in Collections: | IJC Vol.61(11) [Nov 2022] |
Files in This Item:
| File | Description | Size | Format | |
|---|---|---|---|---|
| IJC 61(11) 1184-1187.pdf | 1.6 MB | Adobe PDF | View/Open |
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