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http://nopr.niscpr.res.in/handle/123456789/6780| Title: | An expeditious synthesis of 1,5-benzodiazepine derivatives catalyzed by CdCl2 |
| Authors: | Pasha, M A Jayashankara, V P |
| Keywords: | 2,3-Dihydro-1H-1,5-benzodiazepines;o-phenylenediamine;ketones;CdCl2;solvent-free reaction |
| Issue Date: | Dec-2006 |
| Publisher: | CSIR |
| IPC Code: | Int.Cl.8 C07D |
| Abstract: | 2,3-Dihydro-1H-1,5-benzodiazepines have been synthesized by the condensation of o-phenylenediamine and cyclic or acyclic ketones in the presence of CdCl2 as catalyst at 80-85ºC temperature. The yields are high and the reactions go to completion within 10-20 min. |
| Page(s): | 2716-2719 |
| ISSN: | 0975-0983(Online); 0376-4699(Print) |
| Appears in Collections: | IJC-B Vol.45B(12) December 2006] |
Files in This Item:
| File | Description | Size | Format | |
|---|---|---|---|---|
| IJCB 45B(12) 2716-2719.pdf | 91.81 kB | Adobe PDF | View/Open |
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