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http://nopr.niscpr.res.in/handle/123456789/7072| Title: | Scalable synthesis of 3,4-dihydropyrimidin-2(1H)-ones under solvent free condition |
| Authors: | Kataki, Dolly Chakraborty, Pranita Sarmah, Pubalee Phukan, Prodeep |
| Keywords: | Iodine;Aldehyde;Ethyl acetoacetate;Urea;Dihydropyrimidin-2(1H)-one;Solvent free condition |
| Issue Date: | Sep-2006 |
| Publisher: | CSIR |
| IPC Code: | C07D239/00 |
| Abstract: | An improved solvent free, one pot procedure for the synthesis of 5-ethoxycarbonyl-4-aryl-3,4-dihydropyrimidin-2(1H)-ones catalyzed by iodine is developed. The process has been utilized successfully in large-scale synthesis of Biginelli products. |
| Page(s): | 519-521 |
| ISSN: | 0975-0991 (Online); 0971-457X (Print) |
| Appears in Collections: | IJCT Vol.13(5) [September 2006] |
Files in This Item:
| File | Description | Size | Format | |
|---|---|---|---|---|
| IJCT 13(5) 519-521.pdf | 39.46 kB | Adobe PDF | View/Open |
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