Please use this identifier to cite or link to this item:
http://nopr.niscpr.res.in/handle/123456789/864| Title: | Combustion synthesis of LiMn₂O₄by thermal decomposition of oxalate precursors |
| Authors: | Lagashetty, Arunkumar Havanoor, Vijayanand Basavaraja, S Venkataraman, A |
| Keywords: | Combustion;Synthesis;Morphology;Bonding |
| Issue Date: | Jan-2008 |
| Publisher: | CSIR |
| Abstract: | Self-propagating low temperature combustion method for the synthesis of LiMn₂O₄ is reported. Synthesis of LiMn₂O₄ was carried out by thermal decomposition of lithium oxalate and manganese oxalate precursors employing poly(ethylene glycol) (PEG) as a fuel. The prepared LiMn₂O₄ was then characterized for structure by employing X-ray diffraction (XRD), morphology by scanning electron microscopy (SEM), particle size and shape by transmission electron microscopy (TEM) and bonding by Fourier transform infrared (FT-IR) spectral studies. The powders resulting from this method are pure, spinel-structure LiMn₂O₄ particles of regular shapes. |
| Page(s): | 41-44 |
| ISSN: | 0971–457X |
| Appears in Collections: | IJCT Vol.15(1) [January 2008] |
Files in This Item:
| File | Description | Size | Format | |
|---|---|---|---|---|
| IJCT 15(1) (2008) 41-44.pdf | 414.85 kB | Adobe PDF | View/Open |
Items in NOPR are protected by copyright, with all rights reserved, unless otherwise indicated.