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http://nopr.niscpr.res.in/handle/123456789/46308| Title: | Synthesis and characterization of (cyclopentadienyl)titanium(IV) complexes of 1,3-dihydro-l,3-dioxo-ɑ-substituted)-2H-isoindole 2-acetates |
| Authors: | Saxena, A K Saxena, S Rai, A K |
| Issue Date: | Mar-1990 |
| Publisher: | NISCAIR-CSIR, India |
| Abstract: | Complexes having the general formulae (C5H5)2TiCI(L), (C5H5)TiCI(L)2 and (C5H5)Ti (L)2, have been synthesized by the reactions of N-protected amino acids (LH) , CH(R).CO2H
(where R = - H, - CH(CH3)2, - CH2C6H5, - CH2CH2SCH3 and - CHR - = - CH2CH2- ) with ti-tanocene dichloride in the presence of triethylamine in refluxing tetrahydrofuran. These derivatives have been characterized by elemental analyses, molecular weight measurements, and IR, 1H and 13C NMR spectral studies. |
| Page(s): | 255-259 |
| ISSN: | 0975-0975(Online); 0376-4710(Print) |
| Appears in Collections: | IJC-A Vol.29A(03) [March 1990] |
Files in This Item:
| File | Description | Size | Format | |
|---|---|---|---|---|
| IJCA 29A(3) 255-259.pdf | 299.18 kB | Adobe PDF | View/Open |
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, CH(R).CO2H
(where R = - H, - CH(CH3)2, - CH2C6H5, - CH2CH2SCH3 and - CHR - = - CH2CH2- ) with ti-tanocene dichloride in the presence of triethylamine in refluxing tetrahydrofuran. These derivatives have been characterized by elemental analyses, molecular weight measurements, and IR, 1H and 13C NMR spectral studies.